An Automated Distillation Column for the Unit Operations Laboratory

Authors

  • Douglas M. Perkins Clemson University
  • David A. Bruce Clemson University
  • Charles H. Gooding Clemson University
  • Justin T. Butler Clemson University

Abstract

A batch distillation apparatus has been designed and built for use in the undergraduate unit operations laboratory course. The column is fully automated and is accompanied by data acquisition and control software. A mixture of 1-propanol and 2-propanol is separated in the column, using either a constant distillate rate or constant composition mode of operation. The apparatus allows students to explore distillation and process control topics in an environment that closely resembles industrial practice. 

Author Biographies

Douglas M. Perkins, Clemson University

Douglas M. Perkins is a recent chemical engineering graduate from Clemson University During his undergraduate career he worked closely with Dr. Bruce on designing and building multiple experiments for the Unit Operations Laboratory as well as being the lead student designer/builder of the batch distillation column

David A. Bruce, Clemson University

David A. Bruce is Associate Professor in the Department of Chemical Engineering at Clemson University He earned his BS degrees in Chemistry and Chemical Engineering and his PhD in Inorganic Chemistry from Georgia Institute of Technology His research interests include heterogeneous catalysts with controlled pore geometries. advanced oxidation processes. and quantum and molecular mechanics modeling.

Charles H. Gooding, Clemson University

Charles H. Gooding is Professor of Chemical Engineering at Clemson University He earned his BS and MS degrees at Clemson and his PhD at North Carolina State University, all in chemical engineering. His teaching and research interests are in chemical process design, analysis, and control.

Justin T. Butler, Clemson University

Justin T. Butler is a recent chemical engineering graduate from Clemson University He aided in building/designing the batch column.

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Published

2005-04-01

Issue

Vol. 39 No. 2 (2005): Spring 2005

Section

Manuscripts